Difference between revisions of "CHEM-5181"
From Jimenez Group Wiki
m (→Mass Spectrometers) |
(→Homeworks) |
||
Line 55: | Line 55: | ||
== Homeworks == | == Homeworks == | ||
+ | * [HW10/HW1_2010_Igor_Sector.docx HW1: Igor & Review of Fundamentals] | ||
+ | |||
+ | * [HW10/HW2_TOFMS.docx HW2: TOFMS] | ||
+ | <ul><li><a href="HW10/Raw_TOFAMS_Spec_only.itx">Data for Problem #1</a> (Igor Text File, save and double-click to open in Igor) | ||
+ | </ul> | ||
+ | |||
+ | * [HW10/HW_MS_Resolution.docx">HW 3.1: mass spec resolution and accuracy] | ||
+ | ** [http://cires.colorado.edu/jimenez-group/AMSsd/L_OTH_Q_001_diiodomethane.pxp Quadrupole MS for donwload] (Igor PXP format) | ||
+ | ** [HW10/VLSPYDLTHK.xlsx Orbitrap MS for download] (Excel format) | ||
+ | |||
+ | * [HW10/HW_quadrupole_simul.docx HW3.2: Quadrupole MS simulation] | ||
+ | ** [http://www.jce.divched.org/Journal/Issues/1998/Aug/abs1049.html Understanding the Quadrupole Mass Filter through Computer Simulation], Steel and Henchman, <i>J. Chem. Ed.</i> 75:1049-1054, 1998. | ||
+ | |||
+ | == Labs == | ||
+ | |||
+ | * [http://www.colorado.edu/chemistry/masspec/ Home Page of CU Mass Spec. Facility] | ||
+ | * [http://spreadsheets.google.com/pub?key=rymHDuPsL4R9L5wXigSE5pA&single=true&gid=3&output=html">Lab Schedule for 2010] | ||
+ | |||
+ | * Lab 1: MALDI-TOFMS: | ||
+ | ** [http://www.colorado.edu/chemistry/chem5181/Labs/2010/Voyager_DE_STR catalog.pdf Instrument Description I] | ||
+ | ** [http://www.colorado.edu/chemistry/chem5181/Labs/2010/MALDI_description.pdf Instrument Description II] | ||
+ | ** [http://www.colorado.edu/chemistry/chem5181/Labs/2010/2010_MALDI_Prelab.pdf Pre-Lab] | ||
+ | ** [http://www.colorado.edu/chemistry/chem5181/Labs/2010/2010_MALDI_Lab_Procedure.pdf Lab Procedure] | ||
+ | ** [http://www.colorado.edu/chemistry/chem5181/Labs/2010/MALDI_Instructions_simplified.pdf Instrument Instructions] | ||
+ | |||
+ | * Lab 2: Electrospray MS: | ||
+ | ** [http://www.colorado.edu/chemistry/chem5181/Labs09/2009_ESI_Prelab.pdf Pre-Lab] | ||
+ | ** [http://www.colorado.edu/chemistry/chem5181/Labs09/2009_ESI_lab.pdf Lab] | ||
+ | ** [http://www.colorado.edu/chemistry/chem5181/Labs09/Pulsar_Instructions Pulsar Instrument instructions] | ||
+ | |||
+ | * Lab 3: GC-MS of mixtures | ||
+ | |||
+ | * [http://www.colorado.edu/chemistry/chem5181/Labs/2007_Final_Project.pdf Final Project Organization] | ||
== Labs == | == Labs == |
Revision as of 15:24, 18 November 2010
This is the new home for the CU-Boulder Graduate Course CHEM-5181: Mass Spectrometry and Chromatography
- The old web page is located here, and I'll be gradually move things over to this Wiki page, which is much easier to update.
Contents
Lectures
Introduction, Review, Igor
- Introduction and Review of Fundamentals
- Regression Demo Program (PC Download)
- Non-Parametric Regression Demo (Web)
- Least Squares Polynomial Approximation Demo (Web)
- Central Limit Theorem Demo (Web)
- Fourier Synthesis Demo (Web)
- Fourier Analysis Demo (Web)
Mass Spectrometers
- TOFMS
- Mass Spec. Oscilloscope Simulator (PC Download)
- Sector, FTICR, Orbitrap
- Simulator of Magnetic Sector MS (PC Download)
- 3D Ion Traps
Ionization Sources
- Introduction and Electron Ionization
- Electrospray and its Ion Chemistry (from Invited Lecturer Dr. Shuji Kato)
- Chemical Ionization
- Invited Lecture: the Flowing Afterglow by Prof. Chuck dePuy
- Ionization IV: Bombardment, MALDI and Elemental
Detectors and Data Acquisition
Homeworks
- [HW10/HW1_2010_Igor_Sector.docx HW1: Igor & Review of Fundamentals]
- [HW10/HW2_TOFMS.docx HW2: TOFMS]
- <a href="HW10/Raw_TOFAMS_Spec_only.itx">Data for Problem #1</a> (Igor Text File, save and double-click to open in Igor)
- [HW10/HW_MS_Resolution.docx">HW 3.1: mass spec resolution and accuracy]
- Quadrupole MS for donwload (Igor PXP format)
- [HW10/VLSPYDLTHK.xlsx Orbitrap MS for download] (Excel format)
- [HW10/HW_quadrupole_simul.docx HW3.2: Quadrupole MS simulation]
- Understanding the Quadrupole Mass Filter through Computer Simulation, Steel and Henchman, J. Chem. Ed. 75:1049-1054, 1998.
Labs
- Lab 1: MALDI-TOFMS:
- Lab 2: Electrospray MS:
- Lab 3: GC-MS of mixtures