Difference between revisions of "CHEM-5181"

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=== Detectors and Data Acquisition ===
 
=== Detectors and Data Acquisition ===
  
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* [http://cires.colorado.edu/CHEM-5181/Lect/MS_Detectors_AD_SNR MS Detectors, A/D, Signal-to-Noise]
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* [http://cires.colorado.edu/CHEM-5181/Lect/MS_Detectors_AD_SNR.pdf MS Detectors, A/D, Signal-to-Noise]
 
** ''Props: EMs, MCP''
 
** ''Props: EMs, MCP''
 
** [http://www.vias.org/simulations/simusoft_emultiplier.html Simulation of an Electron Multiplier]
 
** [http://www.vias.org/simulations/simusoft_emultiplier.html Simulation of an Electron Multiplier]

Revision as of 16:25, 7 December 2010

This is the new home for the CU-Boulder Graduate Course CHEM-5181: Mass Spectrometry and Chromatography

  • The old web page is located here, and I'll be gradually move things over to this Wiki page, which is much easier to update.

Course Information

  • This course WILL be offered in Fall 2011, and WILL NOT be offered in Fall 2012
  • Fall 2010 Syllabus
  • Registering for the course:
    • Every CU student attending the course needs to register, either as (a) for grade; (b) for pass/fail; or (c) for "Audit/No Credit".
    • For non-CU students, you can register for the course through the [http://conted.colorado.edu/programs/access/ CU Continuing Education Program ("ACCESS"), again as either (a) for grade; (b) for pass/fail; or (c) for "Audit/No Credit".
  • Lectures: Tue & Thu 11:00-12:15, Ekeley W166
  • Labs: to be determined, based on the student and MS facility schedules (typically three Tue afternoons 1-3 pm)
  • Office hours: immediately after class on Tue & Thu
  • Textbooks:
    • de Hoffmann & Stroobant. Mass Spectrometry, Principles and Applications, 3rd. Ed. ISBN: 0471485667; Library: QD96.M3 H6413 2007
    • McLafferty & Turecek Interpretation of Mass Spectra, 4th Ed., ISBN: 0935702253; Library: QC454.M22 1993;

Lectures

Introduction, Review, Igor

Mass Spectrometers

  • 3D Ion Traps

Ionization Sources

  • Electrospray and its Ion Chemistry (from Invited Lecturer Dr. Shuji Kato)
    • Prop: ESI Source

Detectors and Data Acquisition

MS Interpretation

  • Interpretation of Mass Spectra III (The Molecular Ion)
  • Interpretation of Mass Spectra IV (Fragmentation Mechanisms)

Chromatography and Chemical Separations

Homeworks

Reference material for homeworks

HW on Intro and Review of Fundamentals

HW on TOFMS

HW on Resolution & Accuracy

HW on Quadrupoles

HW on Ion Optics

Labs

Lab 1: MALDI-TOFMS

Lab 2: Electrospray MS

Lab 3: GC-MS of mixtures

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